Efforts to untie the multicollinearity knot and identify factors controlling macropore structures in shale oil reservoirs

Ziyi Wang, Lin Dong, Zhijun Jin, Shuangmei Zou, Jinhua Fu, Rukai Zhu

Abstract view|0|times       PDF download|0|times Supplements download|0|times

Abstract


Traditional correlation analyses based on whole-rock data have limitations in discerning pore development determinants in shale oil reservoir, given the complex lithology of shale formations and intricate interdependencies (multicollinearity) among geological variables. In this study, mercury injection capillary pressure and digital analysis of scanning electron microscopy were employed to examine the macropore structures of both whole rocks and their constituent lithologies for the Upper Triassic Chang-7 shale of the Ordos Basin. Variations were observed among clay shale (shale primarily consisting of clay-sized mineral grains), massive siltstone and silty laminae within the Chang-7 shale. Through the combination of correlation analysis and scanning electron microscope digital technique, it was demonstrated that total organic carbon content primarily controls the level of macropore development, while lithology primarily governs macropore types and structures. Although quartz and pyrite exhibit correlations with macropore volume, they do not emerge as primary factors; instead, they appear interconnected to total organic carbon. Due to detrital mineral framework preservation during compaction, larger macropores are more developed in massive siltstones and silty laminae than in clay shale. Additionally, silty laminae, situated closer to the source rock and influenced by organic acids, exhibit a higher abundance of larger dissolution pores, potentially favoring shale oil development. This study overcomes traditional method constraints, disentangling multi-correlations, and providing new insights into shale macropore development mechanisms, potentially advancing shale oil exploration and production.

Document Type: Original article

Cited as: Wang, Z., Dong, L., Jin, Z., Zou, S., Fu, J., Zhu, R. Efforts to untie the multicollinearity knot and identify factors controlling macropore structures in shale oil reservoirs. Advances in Geo-Energy Research, 2024, 11(3): 194-207. https://doi.org/10.46690/ager.2024.03.04


Keywords


Shale oil reservoir, macropore, controlling factor, multi-lithology, multi-correlation

Full Text:

PDF Supplements

References


Berthonneau, J., Obliger, A., Valdenaire, P. L., et al. Mesoscale structure, mechanics, and transport properties of source rocks’ organic pore networks. Proceedings of the National Academy of Sciences of the United States of America, 2018, 115(49): 12365-12370.

Borjigin, T., Lu, L., Yu, L., et al. Formation, preservation and connectivity control of organic pores in shale. Petroleum Exploration and Development, 2021, 48(4): 798-812.

Cao, Z., Liu, G., Zhan, H., et al. Pore structure characterization of Chang-7 tight sandstone using MICP combined with N2GA techniques and its geological control factors. Scientific Reports, 2016, 6(1): 36919.

Chen, G., Gang, W., Liu, Y., et al. Organic matter enrichment of the Late Triassic Yanchang Formation (Ordos Basin, China) under dysoxic to oxic conditions: Insights from pyrite framboid size distributions. Journal of Asian Earth Sciences, 2019, 170: 106-117.

Cui, J., Zhu, R., Li, S., et al. Development patterns of source rocks in the depression lake basin and its influence on oil accumulation: Case study of the Chang 7 member of the Triassic Yanchang Formation, Ordos Basin, China. Journal of Natural Gas Geoscience, 2019, 4(4): 191-204.

Favilla, S., Durante, C., Vigni, M. L., et al. Assessing feature relevance in NPLS models by VIP. Chemometrics and Intelligent Laboratory Systems, 2013, 129: 76-86.

Fu, J., Li, S., Guo, Q., et al. Enrichment condition and favorable area optimization of continental shale oil in Ordos Basin. Acta Petrolei Sinica, 2022, 43(12): 1702-1716. (in Chinese)

Fu, J., Li, S., Hou, Y., et al. Breakthrough of risk exploration of Class II shale oil in Chang 7 member of Yanchang Formation in the Ordos Basin and its significance. China Petroleum Exploration, 2020, 25(1): 78-92. (in Chinese)

Gao, C., Chen, Y., Yin, J., et al. Experimental study on reservoir characteristics and oil-bearing properties of Chang 7 lacustrine oil shale in Yan’an area, China. Open Geosciences, 2022, 14(1): 234-251.

Goldstein, J. I., Newbury, D. E., Michael, J. R., et al. Scanning Electron Microscopy and X-ray Microanalysis. New York, USA, Springer, 2018.

Guo, H., Jia, W., Peng, P., et al. The composition and its impact on the methane sorption of lacustrine shales from the Upper Triassic Yanchang Formation, Ordos Basin, China. Marine and Petroleum Geology, 2014, 57: 509-520.

Han, H., Liu, P., Ding, Z., et al. The influence of extractable organic matter on pore development in the Late Triassic Chang 7 lacustrine shales, Yanchang Formation, Ordos Basin, China. Acta Geologica Sinica, 2018, 92(4): 1508-1522.

Hu, T., Pang, X., Jiang, F. Advances in whole petroleum system theory and new directions for petroleum geology development. Advances in Geo-Energy Research, 2024, 11(1): 1-5.

Huang, W., Ma, X., Zhou, X., et al. Characteristics and controlling factors of pore structure of shale in the 7th member of Yanchang Formation in Huachi area, Ordos Basin, China. Journal of Natural Gas Geoscience, 2023, 8(5): 319-336.

Khan, D., Qiu, L., Liang, C., et al. Formation and distribution of different pore types in the lacustrine calcareous shale: Insights from XRD, FE-SEM, and low-pressure nitrogen adsorption analyses. ACS Omega, 2022, 7(12): 10820- 10839.

Li, J., Lu, S., Cai, J., et al. Adsorbed and free oil in lacustrine nanoporous shale: A theoretical model and a case study. Energy & Fuels, 2018, 32(12): 12247-12258.

Li, X., Cai, J., Liu, H., et al. Characterization of shale pore structure by successive pretreatments and its significance. Fuel, 2020, 269: 117412.

Lin, S., Hou, L., Luo, X., et al. A millimeter-scale insight into formation mechanism of lacustrine black shale in tephra deposition background. Scientific Reports, 2022, 12(1): 11511.

Liu, J., Li, S., Li, Z., et al. Characteristics and geological significance of pyrite in Chang 73 sub-member in the Ordos Basin. Natural Gas Geoscience, 2021a, 32(12): 1830-1838. (in Chinese)

Liu, K., Ostadhassan, M. Multi-scale fractal analysis of pores in shale rocks. Journal of Applied Geophysics, 2017, 140: 1-10.

Liu, K., Ostadhassan, M., Zhou, J., et al. Nanoscale pore structure characterization of the Bakken shale in the USA. Fuel, 2017, 209: 567-578.

Liu, Q., Li, P., Jin, Z., et al. Preservation of organic matter in shale linked to bacterial sulfate reduction (BSR) and volcanic activity under marine and lacustrine depositional environments. Marine and Petroleum Geology, 2021b, 127: 104950.

Liu, R., Zhou, W., Xu, H., et al. Impact of minerals and sealing systems on the pore characteristics of the Qiongzhusi formation shale in the southern Sichuan Basin. ACS Omega, 2022, 7(18): 15821-15840.

Liu, Y., Shen, B., Yang, Z., et al. Pore structure characterization and the controlling factors of the Bakken Formation. Energies, 2018, 11(11): 2879.

Longman, M., Dahlberg, K., Yared, K. Lithologies and petrophysical characteristics of the Upper Cretaceous Baxter Shale gas reservoir, Canyon Creek Field, Sweetwater County, Wyoming. Paper SPE 180218 Presented at SPE Low Perm Symposium, Denver, Colorado, 5-6 May, 2016.

Lu, H., Xia, D., Li, Q., et al. Quantitative characterization and differences of the pore structure in lacustrine siliceous shale and argillaceous shale: A case study of the Upper Triassic Yanchang Formation shales in the southern Ordos Basin, China. Energy & Fuels, 2021, 35(19): 15525-15544.

Mei, Q., Guo, R., Zhou, X., et al. Pore structure characteristics and impact factors of laminated shale oil reservoir in Chang 73 sub-member of Ordos Basin, China. Journal of Natural Gas Geoscience, 2023, 8(4): 227-243.

Qin, X., Zhao, L., Zhu, J., et al. Modeling the elastic characteristics of overpressure due to thermal maturation in organic shales. Advances in Geo-Energy Research, 2023, 10(3): 174-188.

Qin, Y., Yao, S., Xiao, H., et al. Pore structure and connectivity of tight sandstone reservoirs in petroleum basins: A review and application of new methodologies to the Late Triassic Ordos Basin, China. Marine and Petroleum Geology, 2021, 129: 105084.

Sanei, H. Genesis of solid bitumen. Scientific Reports, 2020, 10: 15595.

Shi, M., Yu, B., Xue, Z., et al. Pore characteristics of organic-rich shales with high thermal maturity: A case study of the Longmaxi gas shale reservoirs from well Yuye-1 in southeastern Chongqing, China. Journal of Natural Gas Science and Engineering, 2015, 26: 948-959.

Sing, K. S., Everett, D. H., Haul, R. A., et al. Reporting physisorption data for gas/solid systems with special reference to the determination of surface area and porosity (Recommendations 1984). Pure and Applied Chemistry, 1985, 57(4): 603-619.

Stocchero, M., Locci, E., d’Aloja, E., et al. PLS2 in metabolomics. Metabolites, 2019, 9(3): 51.

Su, S., Jiang, Z., Xuanlong, S., et al. The effects of shale pore structure and mineral components on shale oil accumulation in the Zhanhua Sag, Jiyang Depression, Bohai Bay Basin, China. Journal of Petroleum Science and Engineering, 2018, 165: 365-374.

Tang, L., Song, Y., Jiang, Z., et al. Influencing factors and mathematical prediction of shale adsorbed gas content in the Upper Triassic Yanchang Formation in the Ordos Basin, China. Minerals, 2019, 9(5): 265.

Wang, G., Jin, Z., Liu, G., et al. Pore system of the multiple lithofacies reservoirs in unconventional lacustrine shale oil formation. International Journal of Coal Geology, 2023a, 273: 104270.

Wang, R., Wang, G., Zhao, G., et al. Geological characteristics and resources potential of shale oil in Chang 7 Member of Upper Triassic Yanchang Formation in Fuxian area, southern Ordos Basin, western China. Unconventional Resources, 2023b, 3: 237-247.

Wang, X., Li, J., Jiang, W., et al. Characteristics, current exploration practices, and prospects of continental shale oil in China. Advances in Geo-Energy Research, 2022, 6(6): 454-459.

Wang, X., Zhu, Y., Chen, S., et al. Molecular structure evaluation and image-guided atomistic representation of marine kerogen from Longmaxi Shale. Energy & Fuels, 2021a, 35(9): 7981-7992.

Wang, Z., Zhang, L., Gao, Y., et al. Pore properties of the lacustrine shale in the upper part of the sha-4 Member of the Paleogene Shahejie Formation in the Dongying Depression in East China. Geofluids, 2021b, 2021: 6616843.

Wold, S., Sjostrom, M., Eriksson, L. PLS-regression: a basic tool of chemometrics. Chemometrics and Intelligent Laboratory Systems, 2001, 58(2): 109-130.

Wu, T., Pan, Z., Liu, B., et al. Laboratory characterization of shale oil storage behavior: A comprehensive review. Energy & Fuels, 2021, 35(9): 7305-7318.

Yan, J., Zhang, S., Wang, J., et al. Applying fractal theory to characterize the pore structure of lacustrine shale from the Zhanhua Depression in Bohai Bay Basin, Eastern China. Energy & Fuels, 2018, 32(7): 7539-7556.

Yang, H., Dou, W., Liu, X., et al. Analysis on sedimentary facies of member 7 in Yanchang Formation of Triassic in Ordos Basin. Acta Sedimentologica Sinica, 2010, 28(2): 254-263. (in Chinese)

Yu, Y., Luo, X., Cheng, M., et al. Study on the distribution of extractable organic matter in pores of lacustrine shale: An example of Zhangjiatan Shale from the Upper Triassic Yanchang Formation, Ordos Basin, China. Interpretation, 2016, 5(2): SF109-SF126.

Yu, Y., Luo, X., Wang, Z., et al. A new correction method for mercury injection capillary pressure (MICP) to characterize the pore structure of shale. Journal of Natural Gas Science and Engineering, 2019, 68: 102896.

Yuan, K., Huang, W., Chen, X., et al. The Whole-aperture pore structure characteristics and their controlling factors of the Dawuba Formation shale in Western Guizhou. Processes, 2022, 10(4): 622.

Zhang, Q., Qiu, Z., Zhang, L., et al. Characteristics and controlling factors of transitional shale gas reservoirs: An example from Permian Shanxi Formation, Daning-Jixian block, Ordos Basin, China. Journal of Natural Gas Geoscience, 2022a, 7(3): 147-157.

Zhang, W., Jin, Z., Liu, Q., et al. The C-S-Fe system evolution reveals organic matter preservation in lacustrine shales of Yanchang Formation, Ordos Basin, China. Marine and Petroleum Geology, 2022b, 142: 105734.

Zhao, W., Hu, S., Hou, L. Connotation and strategic role of insitu conversion processing of shale oil underground in the onshore China. Petroleum Exploration and Development, 2018, 45(4): 563-572.

Zhao, W., Zhu, R., Hu, S., et al. Accumulation contribution differences between lacustrine organic-rich shales and mudstones and their significance in shale oil evaluation. Petroleum Exploration and Development, 2020, 47(6): 1079-1089.




DOI: https://doi.org/10.46690/ager.2024.03.04

Refbacks

  • There are currently no refbacks.


Copyright (c) 2024 The Author(s)

Creative Commons License
This work is licensed under a Creative Commons Attribution-NonCommercial-NoDerivatives 4.0 International License.

Copyright ©2018. All Rights Reserved